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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1268231Generated: October 31, 2026

HCID 18542565, compound → HCID 18542797, compound

https://huagongshe.com/reaction/1268231

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18542565HCID 18542565—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 18542797HCID 18542797100.7%

Reaction Steps

To a solution of 4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3,5-dicarbamoylnitrobenzene (3.0 g) in methanol (60 ml) was added palladium on carbon (0.3 g) and the mixture was stirred under a hydrogen atmosphere at room temperature for 1 hour. The reaction mixture was filtered and the filtrate concentrated in vacuo to give the desired compound (2.8 g, yield quantitative) as a yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06555556B1
Source datasetuspto-grants-2003_04
ORD IDord-ff839399b7544dae83a6f8756712e942
Source noteuspto-grants-2003_04