HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18542565, compound → HCID 18542797, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18542565 | HCID 18542565 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18542797 | HCID 18542797 | 100.7% |
Reaction Steps
To a solution of 4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3,5-dicarbamoylnitrobenzene (3.0 g) in methanol (60 ml) was added palladium on carbon (0.3 g) and the mixture was stirred under a hydrogen atmosphere at room temperature for 1 hour. The reaction mixture was filtered and the filtrate concentrated in vacuo to give the desired compound (2.8 g, yield quantitative) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06555556B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-ff839399b7544dae83a6f8756712e942 |
| Source note | uspto-grants-2003_04 |