HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromoaniline → 1-(4-Bromophenyl)-2-oxo-3-pyrrolidinecarboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromoaniline | HCID 7807 | — |
| Reactant | 1,1-Cyclopropanedicarboxylic acid | HCID 69017 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 1-(4-Bromophenyl)-2-oxo-3-pyrrolidinecarboxylic acid | HCID 3598523 | — |
Reaction Steps
30 g of 1,1-cyclopropanedicarboxylic acid and 50 g of 4-bromoaniline were added to 50 ml of acetonitrile, followed by refluxing for 7 hours with heating and stirring.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06555694B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-8eb52f9df5124485a74cf3eebb8e0392 |
| Source note | uspto-grants-2003_04 |