Hydrochloric Acid → HCID 131726317, compound

Participants

Reaction Steps

137 mg (0.295 mmol) of 2-(3-aminomethylphenylamino)-N-[4-(1,1-dioxoisothiazolidin-2-yl)-3-methylphenyl]-2-phenylacetamide are dissolved in 2.95 ml (0.295 mmol) of 0.1 N HCl in 2-propanol, and the mixture is left to stand at room temperature for 2 hours. The reaction mixture is evaporated and subsequently lyophilised, giving 2-(3-aminomethylphenylamino)-N-[4-(1,1-dioxoisothiazolidin-2-yl)-3-methylphenyl]-2-phenylacetamide, hydrochloride (“BB”) as a colourless solid; ESI 465.

Provenance & Evidence