Piperidine → HCID 69431080, compound
Reaction equation
[O:1]=[C:2]1[C:10]2[C:5](=[CH:6][C:7]([C:11]3[N:12]=[C:13]([CH:22]=O)[NH:14][C:15]=3C3C=CN=CC=3)=[CH:8][CH:9]=2)[CH2:4][CH2:3]1.[NH:24]1[CH2:29][CH2:28][CH2:27][CH2:26][CH2:25]1>>[N:24]1([CH2:22][C:13]2[NH:14][C:15]([C:25]3[CH:26]=[CH:27][CH:28]=[CH:29][N:24]=3)=[C:11]([C:7]3[CH:6]=[C:5]4[C:10](=[CH:9][CH:8]=3)[C:2](=[O:1])[CH2:3][CH2:4]4)[N:12]=2)[CH2:29][CH2:28][CH2:27][CH2:26][CH2:25]1Participants
3
Procedure
The title compound (0.11 g, 44%) was prepared from the product of Step 2 and piperidine as described in Example 6; MS(AP+) m/e 373 [M+H]+.
Sources & evidence
- ORD record
- ord-42acb7bd7891460289aa9eece0249725
- Source dataset
- uspto-grants-2007_04
- Patent number
- US07199137B2
Reaction notes
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