HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 86591437, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 18625989 | HCID 18625989 | — |
| Reactant | HCID 74020541 | HCID 74020541 | — |
| Product | HCID 86591437 | HCID 86591437 | — |
Reaction Steps
The target compound (1.45 g) was obtained as a white powder by carrying out the reaction and the post-treatment according to Reference example 2 using ethyl 2-(4-fluorophenoxy)-3-(4-hydroxyphenyl)propionate (1.8 g) obtained from Reference example 25(b), sodium hydride (55%, 271 mg), and 2-[[1-(4′-fluoro-4-biphenylyl)ethylidene]aminoxy]ethyl methanesulfonate (2.14 g) obtained from Reference example 26(b).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07199139B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-18d5da8321a4460d8bd1850f622bad39 |
| Source note | uspto-grants-2007_04 |