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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1268937Generated: November 1, 2026

Sodium hydride → HCID 86591437, compound

https://huagongshe.com/reaction/1268937

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium hydrideHCID 24758—
ReactantHCID 18625989HCID 18625989—
ReactantHCID 74020541HCID 74020541—
ProductHCID 86591437HCID 86591437—

Reaction Steps

The target compound (1.45 g) was obtained as a white powder by carrying out the reaction and the post-treatment according to Reference example 2 using ethyl 2-(4-fluorophenoxy)-3-(4-hydroxyphenyl)propionate (1.8 g) obtained from Reference example 25(b), sodium hydride (55%, 271 mg), and 2-[[1-(4′-fluoro-4-biphenylyl)ethylidene]aminoxy]ethyl methanesulfonate (2.14 g) obtained from Reference example 26(b).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07199139B2
Source datasetuspto-grants-2007_04
ORD IDord-18d5da8321a4460d8bd1850f622bad39
Source noteuspto-grants-2007_04