HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Trimethylsilyl)ethanol → HCID 91051553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Trimethylsilyl)ethanol | HCID 18013 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 10969049 | HCID 10969049 | — |
| Product | HCID 91051553 | HCID 91051553 | — |
Reaction Steps
The target compound (16.0 g) was obtained as colorless crystals by carrying out the reaction and the post-treatment according to Reference example 20(e) using the above carboxylic acid (13.3 g), oxalyl chloride (18.45 ml) and 2-trimethylsilylethanol (30.3 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07199139B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-67969f1331ef4e4185b62e599d773d21 |
| Source note | uspto-grants-2007_04 |