HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde, 4-(phenylmethoxy)- → HCID 69504523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde, 4-(phenylmethoxy)- | HCID 78109 | — |
| Reactant | HCID 69504410 | HCID 69504410 | — |
| Reactant | HCID 178418657 | HCID 178418657 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 69504523 | HCID 69504523 | — |
Reaction Steps
The target compound (2.68 g) was obtained as a foam by carrying out the reaction and the post-treatment according to Reference example 20(b) using (S)-4-benzyl-3-[(4-fluorophenoxy)acetyl]oxazolidin-2-one (1.96 g) obtained from Reference example 22(a), a solution of dibutylboron triflate in dichloromethane (1M, 7.14 ml), triethylamine (1.08 ml) and 4-benzyloxybenzaldehyde (1.39 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07199139B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-51ca32bcac364123aeb637e7e8d72dd1 |
| Source note | uspto-grants-2007_04 |