HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18448579, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 69427203 | HCID 69427203 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18448579 | HCID 18448579 | — |
Reaction Steps
4-Benzyloxy-2-[(6-hydroxymethyl-1,2,3,4-tetrahydro-naphthalen-1-ylcarbamoyl)-methyl]-pyrrolidine-1-carboxylic acid tert-butyl ester (480 mg. 97 mmol) was dissolved in 25 mL CH2Cl2 and treated with 10 mL TFA and stirred at RT for 15 min, then concentrated to afford the title compound as a colorless glass. (MS,395, M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07199244B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-6ec1d6ce194d496eb6224180ac0d66ca |
| Source note | uspto-grants-2007_04 |