反应详情

Prepared from ethyl (4-{[(2-methoxyethyl)amino]methyl}-2-methylphenoxy)acetate using the synthetic procedure described for Intermediate 45. Purification by Biotage™ chromatography (silica, 90 g) eluted with 100:15 to 100:25 cyclohexane:EtOAc afforded the title compound as a colourless gum (165 mg).

1. customPurification by Biotage™ chromatography (silica, 90 g)
2. washeluted with 100:15 to 100:25 cyclohexane