反应详情

4-iodobenzyl chloride and triethyl phosphite were put in a three-necked flask equipped with a reflux condenser, to which toluene was added and heated with stirring for 8 hours under reflux. The mixture was purified by the common method, to obtain diethyl 4-iodobenzylphosphonate.

1. additionwas added
2. temperatureheated
3. temperatureunder reflux
4. customThe mixture was purified by the common method