HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → Diethyl [(4-iodophenyl)methyl]phosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | 1-(Chloromethyl)-4-iodobenzene | HCID 817211 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Diethyl [(4-iodophenyl)methyl]phosphonate | HCID 15166405 | — |
Reaction Steps
4-iodobenzyl chloride and triethyl phosphite were put in a three-necked flask equipped with a reflux condenser, to which toluene was added and heated with stirring for 8 hours under reflux. The mixture was purified by the common method, to obtain diethyl 4-iodobenzylphosphonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07201976B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-ceaad972f5ef492dba3981f83809dabe |
| Source note | uspto-grants-2007_04 |