HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131726329, compound → HCID 478987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131726329 | HCID 131726329 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 478987 | HCID 478987 | 135.8% |
Reaction Steps
A solution of intermediate 12 (100 mg) in 10% TFA/DCM (1 mL) was stirred at room temperature for 2 h. The solvent was partially evaporated under reduced pressure. For five times the residual was diluted in DCM (2 mL) and concentrated under reduced pressure. Final solvent evaporation afforded the title compound (103.4 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07202221B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-5a477c55854146a89fc224e87623dbd0 |
| Source note | uspto-grants-2007_04 |