HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 69415746, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 69415327 | HCID 69415327 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 69415746 | HCID 69415746 | — |
Reaction Steps
A solution of 1-methoxy-4-(2-pyridin-4-ylethylamino)-[1,2,4]triazolo[4,3-a]quinoxaline-7-carboxylic acid methyl ester (32 mg) was treated with 48% HBr (4 mL) in AcOH (6 mL) at 23° C. After 2 hrs., the solution was concentrated. Trituration of the residue with MeOH/methylene chloride, followed by filtration, afforded a light yellow solid. MS (M+H)+=365.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07202245B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-d915857e429f4379bf651c42e7ee55d8 |
| Source note | uspto-grants-2007_04 |