HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrobenzonitrile → 3-Nitrobenzamidinium hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrobenzonitrile | HCID 12079 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Trimethylaluminum | HCID 16682925 | — |
| Product | 3-Nitrobenzamidinium hydrochloride | HCID 12456162 | — |
Reaction Steps
7.22 g (135 mmol) of ammonium chloride are reacted analogously to example 1A with 135 mmol of trimethylaluminum (67.5 ml of 2 M solution in hexane) and 10 g (67.51 mmol) of 3-nitrobenzonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07202243B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-dd5993f666a54fdfbe29e4972de0a74c |
| Source note | uspto-grants-2007_04 |