Hydrochloric Acid → HCID 11709089, compound

Participants

Reaction Steps

To a mixture of 30.8 g of 2-methyl-3,3,5,5,5-pentafluoro-2,4,4-trihydroxypentyl methacrylate obtained in Example 1 and 300 g of methylene chloride was added 8.7 g of borane-t-butylamine complex, followed by 24 hours of stirring. Dilute hydrochloric acid was added to stop the reaction. Through conventional aqueous work-up and purification by silica gel column chromatography, 26.6 g of the target compound was obtained (yield 91%).

Provenance & Evidence