HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrazole → 1-Phenylpyrazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrazole | HCID 1048 | — |
| Reactant | Bromobenzene | HCID 7961 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 1-Phenylpyrazole | HCID 70769 | — |
Reaction Steps
Operating protocol A (82° C., 24 hours) was followed using 120.8 mg of Chxn-Thio-Al (0.4 mmoles), 211 μl of bromobenzene (2 mmoles), 204 mg of pyrazole (3 mmoles) and 1.2 ml of acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07202367B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-7a49e189cc1d4fc0a2513ee1132f886a |
| Source note | uspto-grants-2007_04 |