HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-1,2,4-Triazole → 1H-1,2,4-Triazole, 1-phenyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-1,2,4-Triazole | HCID 9257 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | Iodobenzene | HCID 11575 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1H-1,2,4-Triazole, 1-phenyl- | HCID 83432 | — |
Reaction Steps
Operating protocol A (82° C., 24 hours) was followed using 117 mg of Chxn-Py-Al (0.4 mmoles), 336 μl of iodobenzene (3 mmoles), 138 mg of 1,2,4-triazole (2 mmoles), 1.042 g of caesium carbonate (3.2 mmoles) and 1.2 ml of DMF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07202367B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-d21407fde4664c9ba4e5cb89aeae7b46 |
| Source note | uspto-grants-2007_04 |