HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonamide → Benzenesulfonanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonamide | HCID 7370 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | Iodobenzene | HCID 11575 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Benzenesulfonanilide | HCID 74296 | — |
Reaction Steps
Example 2.1 was repeated, using 14.4 mg of cuprous oxide (0.1 mmoles), 117 mg of Chxn-Py-Al (0.4 mmoles), 472 mg of benzenesulphonamide (3 mmoles), 224 μl of iodobenzene (2 mmoles), 1.04 g of caesium carbonate (3.2 mmoles), 600 mg of ground and activated 3 Å molecular sieve and 1.6 ml of DMF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07202367B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-b1e2e46933cb42b2a42052ce7504a243 |
| Source note | uspto-grants-2007_04 |