HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Cresol → Benzene, 1,1'-oxybis[methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | 2-Iodotoluene | HCID 5128 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Iodobenzene | HCID 11575 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Benzene, 1,1'-oxybis[methyl- | HCID 78462 | — |
Reaction Steps
Example 3.1 was repeated, replacing the phenol with 206 μl of o-cresol (2 mmoles) and the iodobenzene with 383 μl of 2-iodotoluene (3 mmoles), the acetonitrile with DMF, and with the nucleophile and the arylation agent being added at the same time as the solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07202367B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-d4139118a0e14521a2c0cffc395a74db |
| Source note | uspto-grants-2007_04 |