HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Malonate → Diethyl phenylmalonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Malonate | HCID 7761 | — |
| Reactant | Iodobenzene | HCID 11575 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Diethyl phenylmalonate | HCID 66514 | — |
Reaction Steps
607 μl of diethyl malonate (3 mmoles), 224 μl of iodobenzene (2 mmoles), 1.2 ml of acetonitrile and 600 mg of ground and activated 3 Å molecular sieve were then added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07202367B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-9a371363651944a39408bdca0014876c |
| Source note | uspto-grants-2007_04 |