HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18451515, compound → 7-(Trifluoromethyl)naphthalen-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18451515 | HCID 18451515 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 7-(Trifluoromethyl)naphthalen-2-amine | HCID 18451539 | — |
Reaction Steps
A mixture of 2-nitro-7-trifluoromethylnaphthalene (650 mg, 2.7 mmol) and Raney nickel (65 mg) in methanol (10 mL) is stirred under H2 (1 atm) for 1 hour. Filtration of the catalyst and evaporation of the solvent gives 7-trifluoromethyl-2-aminonaphthalene as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07202364B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-86ee25afe0f3476884fb3ed2bca83084 |
| Source note | uspto-grants-2007_04 |