HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 70573520, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 70567007 | HCID 70567007 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 70573520 | HCID 70573520 | — |
Reaction Steps
To a solution of 0.1 g of 1,9-dioxo-16-hydroxy-1-hydroxymethyl-16-methyl-10,13-trans-prostadiene (Example 1214) in 0.75 ml of pyridine is added 0.026 g of acetic anhydride. After 18 hr. at room temperature, the solvent is removed at reduced pressure and the residue is chromatographed on silica gel to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04254285 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-7235497cc6894fe2855f0536c15a6bda |
| Source note | uspto-grants-1981_03 |