HRID1271234

反应详情

EQUATION

反应方程式

HRID 1271234 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

100.40 g of 4-amino-1-butanol was dissolved in a mixed solvent of 108 ml of acetone and 160 ml of ethanol and, after adding 2.1 g of platinum (IV) oxide, hydrogenation was carried out under the pressure of 2 to 3 atms for 48 hours. A catalyst was removed by filtering the reaction solution and the filtrated was concentrated to obtain 147.64 g of the desired compound as a colorless oily substance.

WORKUP

后处理

  1. customA catalyst was removed
  2. filtrationby filtering the reaction solution
  3. concentrationthe filtrated was concentrated