反应详情

To a solution of 8.60 g of 2-[3-(benzyloxy)phenyl]ethylamine in 50 ml of ethanol, 4.6 ml of ethyl formate was added and the mixture was heated at reflux for 18 hours. The solvent was evaporated under reduced pressure and the residue was purified by silica gel column chromatography to obtain 4.81 g of the desired compound as a pale orange oily substance.

1. temperaturethe mixture was heated
2. temperatureat reflux for 18 hours
3. customThe solvent was evaporated under reduced pressure
4. customthe residue was purified by silica gel column chromatography