Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → 1-[3-(Benzyloxy)phenyl]-2-(formylamino)ethane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | 2-(3-(Benzyloxy)phenyl)ethanamine | HCID 207415 | — |
| 용매 | Ethyl formate | HCID 8025 | — |
| 생성물 | 1-[3-(Benzyloxy)phenyl]-2-(formylamino)ethane | HCID 22931973 | — |
반응 단계
To a solution of 8.60 g of 2-[3-(benzyloxy)phenyl]ethylamine in 50 ml of ethanol, 4.6 ml of ethyl formate was added and the mixture was heated at reflux for 18 hours. The solvent was evaporated under reduced pressure and the residue was purified by silica gel column chromatography to obtain 4.81 g of the desired compound as a pale orange oily substance.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07205302B2 |
| 출처 데이터셋 | uspto-grants-2007_04 |
| ORD ID | ord-8939681e3cad4e74a0f12206f384ff5a |
| 출처 메모 | uspto-grants-2007_04 |