HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Diphenyl-5-(methylamino)pyrazine 1-oxide → 2,3-diphenyl-5-{N-[4-(tert-butoxycarbonylmethoxy)butyl]-N-methylamino}pyrazine 1-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Diphenyl-5-(methylamino)pyrazine 1-oxide | HCID 22932010 | — |
| Reactant | Tert-butyl (4-bromobutyloxy)acetate | HCID 86592459 | — |
| Product | 2,3-diphenyl-5-{N-[4-(tert-butoxycarbonylmethoxy)butyl]-N-methylamino}pyrazine 1-oxide | HCID 22931984 | — |
Reaction Steps
In the same manner as in Example 22, except that 2,3-diphenyl-5-(methylamino)pyrazine 1-oxide was used in place of 5,6-diphenyl-2-(methylamino)pyrazine and 2-(4-bromobutyloxy)acetic acid tert-butyl ester was used in place of 2-(4-bromobutyloxy)acetic acid methyl ester, the desired compound was prepared as a pale yellow oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07205302B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-6f65e69dfaf445298e4979cdcbd0bc42 |
| Source note | uspto-grants-2007_04 |