HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,5-Diphenyl-2-(methylamino)pyrimidine → 2-{4-[N-(4,5-diphenylpyrimidin-2-yl)-N-methylamino]butyloxy}acetic Acid Tert-Butyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,5-Diphenyl-2-(methylamino)pyrimidine | HCID 22931975 | — |
| Reactant | Tert-butyl (4-bromobutyloxy)acetate | HCID 86592459 | — |
| Product | 2-{4-[N-(4,5-diphenylpyrimidin-2-yl)-N-methylamino]butyloxy}acetic Acid Tert-Butyl Ester | HCID 69354678 | — |
Reaction Steps
In the same manner as in Example 22, except that 4,5-diphenyl-2-(methylamino)pyrimidine was used in place of 5,6-diphenyl-2-(methylamino)pyrazine and 2-(4-bromobutyloxy)acetic acid tert-butyl ester was used in place of 2-(4-bromobutyloxy)acetic acid methyl ester, the desired compound was prepared as a pale yellow oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07205302B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-5d0a30ff279f4122bf24419a1ca132f3 |
| Source note | uspto-grants-2007_04 |