HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68588179, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 68586368 | HCID 68586368 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 68588179 | HCID 68588179 | — |
Reaction Steps
The material from step B (350 mg, 0.71 mmol) was treated with ethyl acetate saturated with hydrogen chloride (7 mL) for 4 hours at room temperature. The mixture was concentrated in vacuo to afford, after trituration with ethyl acetate and diethyl ether, the desired aminoacid (250 mg, 82%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07205313B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-047a611befbd44d39ed7828ff29dfb4e |
| Source note | uspto-grants-2007_04 |