HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68588477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86640932 | HCID 86640932 | — |
| Product | HCID 68588477 | HCID 68588477 | 96% |
Reaction Steps
The alkylated decahydroisoquinoline derivative from step C (36 mg, 0.075 mmol) was treated with 6M hydrochloric acid under reflux for 35 h. The solution was concentrated in vacuo and water added and concentrated in vacuo (3×), followed by addition of acetone and concentration in vacuo (3×), to give an off-white solid (30 mg, 96% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07205313B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-dc6d1ae3aa2043a097571158ec2b032c |
| Source note | uspto-grants-2007_04 |