Hydrochloric Acid → HCID 68585653, compound

HRID 1271514Notes

Reaction equation

C([O:3][C:4]([C:6]1[CH:11]=[CH:10][C:9]([CH3:12])=[CH:8][C:7]=1[S:13][C@H:14]1[CH2:23][CH2:22][C@@H:21]2[C@@H:16]([CH2:17][C@@H:18]([C:28]([O:30]CC)=[O:29])[N:19](C(OC)=O)[CH2:20]2)[CH2:15]1)=[O:5])C.[ClH:33]>>[ClH:33].[C:4]([C:6]1[CH:11]=[CH:10][C:9]([CH3:12])=[CH:8][C:7]=1[S:13][C@H:14]1[CH2:23][CH2:22][C@@H:21]2[C@@H:16]([CH2:17][C@@H:18]([C:28]([OH:30])=[O:29])[NH:19][CH2:20]2)[CH2:15]1)([OH:5])=[O:3]

Participants

Reactant 2

HCID 313Hydrochloric Acid

HCID 86640933HCID 86640933, compound

Product 1

HCID 68585653HCID 68585653, compoundYield 84%

Procedure

Following the procedures for Example 22, Step D, extensive hydrolysis of material from step C (54 mg, 0.12 mmol) with 6M hydrochloric acid (3 mL) gave the title product (39 mg, 84% yield).

Sources & evidence

ORD record: ord-73ef2f3981ad46dd8599accf505831c5
Source dataset: uspto-grants-2007_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07205313B2

Reaction notes

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