Hydrochloric Acid → HCID 18454779, compound

Participants

Reaction Steps

(6-methyl-2-phenylethynyl-pyridin-3-yl)amine (105 mg, 0.50 mmol) was dissolved in CHCl3 (2 ml) and treated with 1.56 ml (1.25 mmol) of 0.8 M hydrochloric acid solution in diethyl ether. After evaporation of the solvent and trituration of the residue with ethyl acetate, 107 mg (0.44 mmol, 87%) of the title hydrochloride were obtained as a yellowish solid.

Provenance & Evidence