HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69418848, compound → HCID 131726335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69418848 | HCID 69418848 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131726335 | HCID 131726335 | — |
Reaction Steps
A solution of 2-(2-(S)-cyano-pyrrolidine-1-carbonyl)-5-(R/S)-(2-m-tolyl-vinyl)-pyrrolidine-1-carboxylic acid tert-butyl ester (Example 23) (50 mg) and 10% Pd/C(10 mg) in ethanol (5mL) was stirred under H2 balloon overnight. The catalyst was removed by filtration, and the filtrate was concentrated to provide the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07205409B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-4e7b1cfa34df45968690a55102097343 |
| Source note | uspto-grants-2007_04 |