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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1271785Generated: November 2, 2026

Hydrazine → HCID 22131447, compound

https://huagongshe.com/reaction/1271785

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazineHCID 9321—
ReactantHCID 22131444HCID 22131444—
SolventEthanolHCID 702—
ProductHCID 22131447HCID 22131447107.2%

Reaction Steps

N-(2-quinolyl)methoxy phthalimide (782 mg) was suspended in 95% EtOH and hydrazine (0.15 mL) was added. The reaction mixture was stirred overnight and then filtered. The filtrate was concentrated under reduced pressure and then taken up in a small amount of dichloromethane. The small amount of remaining phthalhydrazide was then removed by filtration. The filtrate was concentrated under reduced pressure to give the title compound (480 mg) as a yellow oil. MS(CI) m/e 175 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUSRE039591E1
Source datasetuspto-grants-2007_04
ORD IDord-164d1679b693489594483b88ee377c1e
Source noteuspto-grants-2007_04