HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 22131447, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 22131444 | HCID 22131444 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22131447 | HCID 22131447 | 107.2% |
Reaction Steps
N-(2-quinolyl)methoxy phthalimide (782 mg) was suspended in 95% EtOH and hydrazine (0.15 mL) was added. The reaction mixture was stirred overnight and then filtered. The filtrate was concentrated under reduced pressure and then taken up in a small amount of dichloromethane. The small amount of remaining phthalhydrazide was then removed by filtration. The filtrate was concentrated under reduced pressure to give the title compound (480 mg) as a yellow oil. MS(CI) m/e 175 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE039591E1 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-164d1679b693489594483b88ee377c1e |
| Source note | uspto-grants-2007_04 |