HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-[2,4-bis(phenylmethoxy)phenyl]-2,2,2-trifluoroacetamide → N-(2,4-dihydroxyphenyl)-2,2,2-trifluoro-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-[2,4-bis(phenylmethoxy)phenyl]-2,2,2-trifluoroacetamide | HCID 18454995 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(2,4-dihydroxyphenyl)-2,2,2-trifluoro-acetamide | HCID 18454996 | — |
Reaction Steps
A mixture of 1.5 grams (0.0036 mole) of, N-[2,4-bis(phenylmethoxy)phenyl]-2,2,2-trifluoroacetamide and 0.2 gram (catalyst) of 10% palladium on carbon in 125 mL of ethanol was treated with hydrogen gas in a Parr Hydrogenator, yielding 0.80 gram of the subject compound. The NMR spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07208450B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-5f443e488cd747bfbbdd4750efefd45d |
| Source note | uspto-grants-2007_04 |