HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyridine → Acetic acid (4-methoxy-phenyl)-(pyridin-2-ylcarbamoyl)-methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | Acetoxy-(4-methoxy-phenyl)-acetic acid | HCID 18456650 | — |
| Product | Acetic acid (4-methoxy-phenyl)-(pyridin-2-ylcarbamoyl)-methyl ester | HCID 58847454 | — |
Reaction Steps
was prepared from intermediate 79a and 2-aminopyridine following Method A. 1H NMR (300 MHz, CDCl3) δ 9.06 (s, 1H), 8.31–8.23 (m, 2H), 7.81–7.75 (m, 1H), 7.43 (d, 2H, J=8.59 Hz), 6.90 (d, 2H, J=8.59 Hz), 6.14 (s, 1H), 3.79 (s, 3H), 2.25 (s, 3H). LCMS (ESI+) [M+H]/z Calc'd 301, found 301.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07208500B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-fd9e861b76b74a6f8af44b1dfaa4e571 |
| Source note | uspto-grants-2007_04 |