Methyl Isocyanate → HCID 86737558, compound

Participants

Reaction Steps

2-oxo-4-phenyl-5,5-dimethyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4-phenyl-5,5-dimethyl-3-thiazoline-O-(methylcarbamoyl)-oxime, m.p. 135°-137° C. The 2-oxo-4-phenyl-5,5-dimethyl-3-thiazoline-oxime starting material (m.p. 147°-149° C.) was prepared from 2-methyl-1-phenyl-2-thiocyanato-1-propanone (b.p. [0.02 mm] 98°-100° C.).

Provenance & Evidence