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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1272178Generated: October 30, 2026

Di-tert-butyl dicarbonate → HCID 69360303, compound

https://huagongshe.com/reaction/1272178

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDi-tert-butyl dicarbonateHCID 90495—
ReactantHCID 18455988HCID 18455988—
ReactantAluminium lithium hydrideHCID 21226445—
ReactantHCID 69357759HCID 69357759—
Catalyst4-(Dimethylamino)pyridineHCID 14284—
ProductHCID 69360303HCID 69360303—

Reaction Steps

This compound was prepared in analogy to Example 1, intermediate h) from 7-ethoxy-4-methyl-3,4-dihydro-2H-2,4a,5-triaza-fluoren-1-one and lithium aluminium hydride and protection of the free amine with di-tert-butyl-dicarbonate and 4-(dimethylamino)pyridine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07208494B2
Source datasetuspto-grants-2007_04
ORD IDord-e5c7fdb207e345fca1bea6bef1614321
Source noteuspto-grants-2007_04