HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20286520, compound → HCID 20286537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20286520 | HCID 20286520 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20286537 | HCID 20286537 | 100.9% |
Reaction Steps
A mixture of 4.54 g 4,4-dimethyl-8-carbobenzyloxy-1-oxa-3,8-diazaspiro[4.5]decan-2-one, 75 ml ethanol and 1 g 5% palladium on carbon is hydrogenated at 60 psi and 50° for one hour. Filtration and evaporation affords 2.65 g 4,4-dimethyl-1-oxa-3,8-diazaspiro[4.5]decan-2-one, mp 238°-240°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04255432 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-fa909dfbfbfb410cb9ec7d0466b15559 |
| Source note | uspto-grants-1981_03 |