HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21923012, compound → HCID 18457583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21923012 | HCID 21923012 | — |
| Reactant | HCID 178511674 | HCID 178511674 | — |
| Product | HCID 18457583 | HCID 18457583 | 1,240.1% |
Reaction Steps
The operation is carried out as in Stage 3 of Example 9 starting from 27.9 mg of the product obtained in Stage 1 above and 720 mg of trans-1,4-diaminocyclohexane. After purification under the same conditions as for Example 9, salification is carried out with 10 ml 1.4N HCl/Ethanol followed by evaporating to dryness. In this way 232 mg of expected product is obtained in the form of crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07208598B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-326ddc03bed04cb482d9aca8780823b5 |
| Source note | uspto-grants-2007_04 |