HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Benzyloxyaniline → HCID 70269237, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Benzyloxyaniline | HCID 22860 | — |
| Reactant | 2-Chloro-6,7-dimethoxy-4-quinazolinamine | HCID 90235 | — |
| Product | HCID 70269237 | HCID 70269237 | — |
Reaction Steps
2-chloro-6,7-dimethoxy-4-quinazolinamine (1.73 g, 7 mmol) and 4-benzyloxyaniline (2.5 g, 12 mmol) were heated in an s.s. bomb at 145° C. for 16 hrs. Upon cooling the resultant solid was washed well with ether to afford the product. 1H NMR DMSO 3.86 (d, 6H , OCH3), 5.14 (s, 2H, CH2), 6.9-7.5 (m, 11H, ArH)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06156758 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-044c75698b07478599b03a0ce5ac87a0 |
| Source note | uspto-grants-2000_12 |