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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1274158Generated: November 3, 2026

4-Benzyloxyaniline → HCID 70269237, compound

https://huagongshe.com/reaction/1274158

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-BenzyloxyanilineHCID 22860—
Reactant2-Chloro-6,7-dimethoxy-4-quinazolinamineHCID 90235—
ProductHCID 70269237HCID 70269237—

Reaction Steps

2-chloro-6,7-dimethoxy-4-quinazolinamine (1.73 g, 7 mmol) and 4-benzyloxyaniline (2.5 g, 12 mmol) were heated in an s.s. bomb at 145° C. for 16 hrs. Upon cooling the resultant solid was washed well with ether to afford the product. 1H NMR DMSO 3.86 (d, 6H , OCH3), 5.14 (s, 2H, CH2), 6.9-7.5 (m, 11H, ArH)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06156758
Source datasetuspto-grants-2000_12
ORD IDord-044c75698b07478599b03a0ce5ac87a0
Source noteuspto-grants-2000_12