Methanol → HCID 22120786, compound

Participants

Reaction Steps

The title compound was prepared from 2-[5-(1,2,3-triazol-1-ylmethyl)thien-2-yl]-N-[2-(acetylthiomethyl)-4-phenylbutyryl]glycine ethyl ester (Description 57) by the procedure described in Example 24 except that the eluent used was 20% methanol indichloromethane. vmax (CHCl3) 3292, 1731, 1648 and 1602 cm-1. δ (CD3SOCD3) 1.70-1.82 (2H, m), 2.46-2.74 (5H, m), 5.22 (1H, d, J 6.85 Hz), 5.72 (2H, s), 6.85-7.31 (7H, m), 7.68 and 7.72 (1H, two s's), 8.11 and 8.14 (1H, two s's).

Provenance & Evidence