HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22120830, compound → HCID 22120826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22120830 | HCID 22120830 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 22120826 | HCID 22120826 | — |
Reaction Steps
The title compound was prepared from 2-[5-(1,2,3-triazol-2-ylmethyl)thien-2-yl]-N-[2-(acetylthiomethyl)-4-phenylbutyryl]glycine ethyl ester by (Description 59) the procedure described in Example 29. vmax (CHCl3) 3289 and 1621 cm-1. δ (CD3SOCD3) 1.68-1.83 (2H, m), 2.44-2.73 (5H, m), 5.20 (1H, d, J 6.87 Hz), 5.73 (2H, s), 6.83-6.94 (2H, m), 7.10-7.30 (5H, m), 7.74 and 7.78 (2H, two s's), 8.10 (1H, d, J 7.07 Hz). m/z 431 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06156774 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-25a151ceda0a46128889879813357c03 |
| Source note | uspto-grants-2000_12 |