Potassium Bromide → HCID 22120868, compound

HRID 1274232Notes

Reaction equation

C([O:3][C:4](=[O:36])[CH:5]([C:23]1[S:24][C:25]([CH2:28][N:29]2[C:33](=[O:34])[CH2:32][NH:31][C:30]2=[O:35])=[CH:26][CH:27]=1)[NH:6][C:7](=[O:22])[CH:8]([CH2:17][S:18]C(=O)C)[CH2:9][CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)C.[K+].[Br-]>>[NH:31]1[CH2:32][C:33](=[O:34])[N:29]([CH2:28][C:25]2[S:24][C:23]([CH:5]([C:4]([OH:36])=[O:3])[NH:6][C:7](=[O:22])[CH:8]([CH2:17][SH:18])[CH2:9][CH2:10][C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=3)=[CH:27][CH:26]=2)[C:30]1=[O:35]

Participants

Reactant 2

HCID 253877Potassium Bromide

HCID 22120837HCID 22120837, compound

Product 1

HCID 22120868HCID 22120868, compound

Procedure

The title compound was prepared from 2-[5-(imidazolidin-2,4-dion-3-ylmethyl)thien-2-yl]-N-[2-(acetylthiomethyl)-4-phenylbutyryl]glycine ethyl ester (Description 62) by the procedure described in Example 27. vmax (KBr) 3391, 1714 and 1638 cm-1. m/z 479 (MNH4+).

Sources & evidence

ORD record: ord-263b74432ee74eb58580997e1337b290
Source dataset: uspto-grants-2000_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06156774

Reaction notes

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