HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22120930, compound → HCID 22120928, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22120930 | HCID 22120930 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22120928 | HCID 22120928 | — |
Reaction Steps
The title compound was prepared from 1-acetyl-5-(1-azabicyclo[3.3.1]non-3-en-4-yl)methoxy-6-bromo-2,3-dihydro-1H-indole (D9) by a similar procedure to Description 4 using toluene as solvent. The two isomers (2:1 ratio) formed around the spirocyclic junction were separated by column chromatography on silica gel eluting with 0-15% methanol/chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06156783 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-e0221adaecfc42b3856477a7b720c91d |
| Source note | uspto-grants-2000_12 |