Isopropanol → HCID 131722196, compound

HRID 1274373Notes

Reaction equation

HRID 1274373 reaction equation
[CH:1]1[CH:6]=[C:5]([CH2:7][NH2:8])[CH:4]=[C:3]([CH2:9][NH2:10])[CH:2]=1.[CH3:11][CH:12]([OH:14])[CH3:13]>O>[CH:1]1[CH:6]=[C:5]([CH2:7][NH2:8])[CH:4]=[C:3]([CH2:9][NH2:10])[CH:2]=1.[CH3:11][CH:12]([OH:14])[CH3:13]

Participants

4

Reactant 2

HCID 3776IsopropanolHCID 151331,3-Benzenedimethanamine

Product 1

HCID 131722196HCID 131722196, compoundYield 144.6%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
90 °C

Procedure

1440 g of MXDA and 1750 g of IPA were mixed with 3.0 kg of water and stirred at 90° C. for 1 hour. After becoming clear, the mixture solution was cooled to 25° C. The precipitate was then isolated by decantation, and vacuum dried at 25° C. for 24hours. 3.0 kg of MXDA/IPA salt was thus obtained.

Workup

  1. temperaturethe mixture solution was cooled to 25° C
  2. customThe precipitate was then isolated by decantation, and vacuum
  3. customdried at 25° C. for 24hours

Sources & evidence

ORD record
ord-dcac702c18714dbe9983a082fabcefd8
Source dataset
uspto-grants-2000_12
Patent number
US06156838

Reaction notes

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