HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Dimethylthiourea → HCID 20638585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Dimethylthiourea | HCID 2723631 | — |
| Reactant | HCID 20638585 | HCID 20638585 | — |
| Reactant | 2-Bromo-6-tert-butyl-2,3-dihydro-1H-inden-1-one | HCID 22119032 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20638585 | HCID 20638585 | — |
| Product | HCID 20638586 | HCID 20638586 | — |
Reaction Steps
5-tert-Butyl-3-methyl-2-methylimino-2,3,8,8a-tetrahydroindeno-[1,2-d]thiazol-3a-ol hydrobromide: The reaction of 267 mg of 2-bromo-6-tert-butylindan-1-one with 156 mg of N,N'-dimethylthiourea in 10 ml of acetone yields the hydrobromide of 5-tert-butyl-3-methyl-2-methylimino-2,3,8,8a-tetrahydroindeno[1,2-d]thiazol-3a-ol of melting point 277-279° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06159996 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-274588fa05694805a082778122effffa |
| Source note | uspto-grants-2000_12 |