Hydrazine hydrate (1:1) → Benzyl carbazate

HRID 1275414Notes

Reaction equation

HRID 1275414 reaction equation
[C:1](=O)([O:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[O:2]CC1C=CC=CC=1.O.[NH2:20][NH2:21]>>[C:1]([O:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)(=[O:2])[NH:20][NH2:21]

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 77002Carbonic acid, bis(phenylmethyl) ester

Product 1

HCID 79242Benzyl carbazate

Procedure

The 2nd step is carried out analogously in further experiments B, C, and D at room temperature using the dibenzyl carbonate and hydrazine hydrate ratios given in Table 1. The amount and purity of benzyl carbazate that is obtained are likewise summarized in Table 1.

Workup

  1. customis carried out analogously in further experiments B, C, and D at room temperature

Sources & evidence

ORD record
ord-0eba60316d0445648e2e1d45256c3f64
Source dataset
uspto-grants-2000_12
Patent number
US06160160

Reaction notes

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