HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 6-(2',5'-dimethylphenyl)-5-keto-3,3-dimethylhexanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 6-(2',5'-Dimethylphenyl)-5-keto-3,3-dimethyl hexanoic acid | HCID 13688124 | — |
| Product | Ethyl 6-(2',5'-dimethylphenyl)-5-keto-3,3-dimethylhexanoate | HCID 13688125 | 78% |
Reaction Steps
Utilizing the procedure of EXAMPLE XX 6-(2',5'-dimethylphenyl)-5-keto-3,3-dimethyl hexanoic acid was esterified with absolute ethanol in the presence of a catalytic amount of concentrated sulfuric acid to provide 15.52 g (78% yield) of ethyl 6-(2',5'-dimethylphenyl)-5-keto-3,3-dimethylhexanoate as a pale viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04256659 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-d30bd00a4f2d44b49a8bf4d70986adbe |
| Source note | uspto-grants-1981_03 |