Ethanol → Tetradecylamine

HRID 1275480Notes

Reaction equation

HRID 1275480 reaction equation
[CH2:1](O)[CH3:2].[CH2:4]([NH2:16])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]>O>[CH2:4]([NH2:16])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:1][CH3:2]

Participants

4

Reactant 2

HCID 702EthanolHCID 13583Dodecylamine

Product 1

HCID 16217Tetradecylamine

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

In application Ser. No. 355,979, filed Dec. 14, 1994, describing the assembly of silica molecular sieves in 50:50 (v/v) water:ethanol, it was shown that certain alkylamine surfactants (e.g., dodecylamine) gave derivatives with high textural mesoporosity whereas others afforded relatively low textural pore volumes (e.g., tetradecylamine (Tanev, P.

Workup

  1. customgave derivatives with high textural mesoporosity whereas others

Sources & evidence

ORD record
ord-587abae7cbef47b099d17be0f0a84e38
Source dataset
uspto-grants-2000_12
Patent number
US06162414

Reaction notes

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