Hydrogen Peroxide → HCID 22117088, compound

HRID 1275535Notes

Reaction equation

HRID 1275535 reaction equation
S(=O)(=O)(O)O.OO.[OH-].[Na+].[C:10]([N:23]([CH2:25][C:26]([O-:28])=[O:27])[CH3:24])(=[O:22])[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21].[Na+].[Co:30]>>[C:10]([N:23]([CH2:25][C:26]([O-:28])=[O:27])[CH3:24])(=[O:22])[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21].[Co+2:30].[C:10]([N:23]([CH2:25][C:26]([O-:28])=[O:27])[CH3:24])(=[O:22])[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]

Participants

6

Reactant 5

HCID 784Hydrogen Peroxide2×HCID 1118Sulfuric AcidHCID 14798Sodium HydroxideHCID 104730CobaltHCID 23668817Glycine, N-methyl-N-(1-oxododecyl)-, sodium salt

Product 1

HCID 22117088HCID 22117088, compound

Procedure

1000 ml of the cobalt solution resulting from separation of the organic phase and containing sulfuric acid, residues of hydrogen peroxide and 0.98% by weight of Co are adjusted to a pH of 6.5 by addition of about 130 g of 18% strength by weight sodium hydroxide solution and subsequently freed of hydrogen peroxide by heating to the boiling point. 333 ml of aqueous 1M sodium N-lauroylsarcosinate are subsequently added, forming cobalt N-lauroylsarcosinate in the form of a pale pink precipitate.

Workup

  1. temperatureby heating to the boiling point

Sources & evidence

ORD record
ord-98b7895e8909439fa657f5e58403cce5
Source dataset
uspto-grants-2000_12
Patent number
US06162753

Reaction notes

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